固(gu)(gu)(gu)溶(rong)(rong)處(chu)(chu)理(li)(li)是(shi)將合(he)(he)(he)金(jin)(jin)(jin)加(jia)熱到高(gao)(gao)溫(wen)(wen)(wen)單(dan)-相(xiang)區恒溫(wen)(wen)(wen)保(bao)持,使(shi)(shi)過(guo)(guo)剩相(xiang)溶(rong)(rong)解(jie)(jie)到溶(rong)(rong)體后快(kuai)速(su)冷卻(que)、以(yi)(yi)得(de)到過(guo)(guo)飽(bao)和(he)(he)(he)固(gu)(gu)(gu)溶(rong)(rong)體的(de)(de)(de)(de)(de)(de)熱處(chu)(chu)理(li)(li)工藝。首先,固(gu)(gu)(gu)溶(rong)(rong)處(chu)(chu)理(li)(li)是(shi)為了(le)溶(rong)(rong)解(jie)(jie)基體內碳化物、γ'相(xiang)等以(yi)(yi)得(de)到均(jun)勻的(de)(de)(de)(de)(de)(de)過(guo)(guo)飽(bao)和(he)(he)(he)固(gu)(gu)(gu)溶(rong)(rong)體,便于(yu)(yu)時(shi)效時(shi)重新析(xi)出顆(ke)粒細(xi)小、分布均(jun)勻的(de)(de)(de)(de)(de)(de)碳化物和(he)(he)(he)γ'等強(qiang)化相(xiang),同時(shi)消除由于(yu)(yu)冷熱加(jia)工產生的(de)(de)(de)(de)(de)(de)應(ying)力。使(shi)(shi)合(he)(he)(he)金(jin)(jin)(jin)發生再結晶。其次(ci),固(gu)(gu)(gu)溶(rong)(rong)處(chu)(chu)理(li)(li)是(shi)為了(le)獲(huo)得(de)適宜的(de)(de)(de)(de)(de)(de)晶粒度(du)(du)(du),以(yi)(yi)保(bao)證合(he)(he)(he)金(jin)(jin)(jin)高(gao)(gao)溫(wen)(wen)(wen)抗蠕(ru)變(bian)(bian)性能。固(gu)(gu)(gu)溶(rong)(rong)處(chu)(chu)理(li)(li)的(de)(de)(de)(de)(de)(de)溫(wen)(wen)(wen)度(du)(du)(du)范圍為980~1250℃,主(zhu)要(yao)根據各(ge)個(ge)合(he)(he)(he)金(jin)(jin)(jin)中相(xiang)析(xi)出和(he)(he)(he)溶(rong)(rong)解(jie)(jie)規律及(ji)使(shi)(shi)用要(yao)求(qiu)來選(xuan)擇,以(yi)(yi)保(bao)證主(zhu)要(yao)強(qiang)化相(xiang)必要(yao)的(de)(de)(de)(de)(de)(de)析(xi)出條件和(he)(he)(he)一定的(de)(de)(de)(de)(de)(de)晶粒度(du)(du)(du)。對于(yu)(yu)長(chang)期高(gao)(gao)溫(wen)(wen)(wen)使(shi)(shi)用的(de)(de)(de)(de)(de)(de)合(he)(he)(he)金(jin)(jin)(jin),要(yao)求(qiu)有(you)較(jiao)好的(de)(de)(de)(de)(de)(de)高(gao)(gao)溫(wen)(wen)(wen)持久和(he)(he)(he)蠕(ru)變(bian)(bian)性能,應(ying)選(xuan)擇較(jiao)高(gao)(gao)的(de)(de)(de)(de)(de)(de)固(gu)(gu)(gu)溶(rong)(rong)溫(wen)(wen)(wen)度(du)(du)(du)以(yi)(yi)獲(huo)得(de)較(jiao)大的(de)(de)(de)(de)(de)(de)晶粒度(du)(du)(du);對于(yu)(yu)中溫(wen)(wen)(wen)使(shi)(shi)用并要(yao)求(qiu)較(jiao)好的(de)(de)(de)(de)(de)(de)室溫(wen)(wen)(wen)硬度(du)(du)(du)、屈服強(qiang)度(du)(du)(du)、拉伸強(qiang)度(du)(du)(du)、沖擊韌性和(he)(he)(he)疲勞(lao)強(qiang)度(du)(du)(du)的(de)(de)(de)(de)(de)(de)合(he)(he)(he)金(jin)(jin)(jin),可采(cai)用較(jiao)低的(de)(de)(de)(de)(de)(de)固(gu)(gu)(gu)溶(rong)(rong)溫(wen)(wen)(wen)度(du)(du)(du),保(bao)證較(jiao)小的(de)(de)(de)(de)(de)(de)晶粒度(du)(du)(du)。高(gao)(gao)溫(wen)(wen)(wen)固(gu)(gu)(gu)溶(rong)(rong)處(chu)(chu)理(li)(li)時(shi),各(ge)種析(xi)出相(xiang)都逐步(bu)溶(rong)(rong)解(jie)(jie),同時(shi)晶粒長(chang)大;低溫(wen)(wen)(wen)固(gu)(gu)(gu)溶(rong)(rong)處(chu)(chu)理(li)(li)時(shi),不僅有(you)主(zhu)要(yao)強(qiang)化相(xiang)的(de)(de)(de)(de)(de)(de)溶(rong)(rong)解(jie)(jie),而(er)且可能有(you)某些相(xiang)的(de)(de)(de)(de)(de)(de)析(xi)出。對于(yu)(yu)過(guo)(guo)飽(bao)和(he)(he)(he)度(du)(du)(du)低的(de)(de)(de)(de)(de)(de)合(he)(he)(he)金(jin)(jin)(jin),通常選(xuan)擇較(jiao)快(kuai)的(de)(de)(de)(de)(de)(de)冷卻(que)速(su)度(du)(du)(du);對于(yu)(yu)過(guo)(guo)飽(bao)和(he)(he)(he)度(du)(du)(du)高(gao)(gao)的(de)(de)(de)(de)(de)(de)合(he)(he)(he)金(jin)(jin)(jin),通常為空氣中冷卻(que)。
對2205雙(shuang)相(xiang)不銹鋼(gang)進行不同溫度的固溶處理會導致2205雙相不銹鋼兩相組織的改變,進而導致其性能的差異,圖3.1是在不同溫度下2205雙相不銹鋼固溶處理后的微觀組織。


選取(qu)1000℃作為(wei)最低(di)固(gu)溶溫(wen)(wen)度,當(dang)熱處理溫(wen)(wen)度低(di)于(yu)950℃時(shi),雙(shuang)相(xiang)(xiang)(xiang)不銹鋼(gang)基體(ti)(ti)(ti)會(hui)析出雜質相(xiang)(xiang)(xiang)σ相(xiang)(xiang)(xiang),σ相(xiang)(xiang)(xiang)作為(wei)富含Cr、Mo的(de)硬脆相(xiang)(xiang)(xiang),其存在(zai)降低(di)雙(shuang)相(xiang)(xiang)(xiang)不銹鋼(gang)的(de)耐蝕性能。圖3.1(a)為(wei)950℃的(de)微(wei)觀組織,。相(xiang)(xiang)(xiang)廣泛分(fen)布(bu)于(yu)鐵素(su)(su)體(ti)(ti)(ti)/奧(ao)氏體(ti)(ti)(ti)晶界。當(dang)溫(wen)(wen)度達到(dao)1000℃時(shi),σ相(xiang)(xiang)(xiang)會(hui)消失,雙(shuang)相(xiang)(xiang)(xiang)不銹鋼(gang)中(zhong)只存在(zai)鐵素(su)(su)體(ti)(ti)(ti)相(xiang)(xiang)(xiang)和奧(ao)氏體(ti)(ti)(ti)相(xiang)(xiang)(xiang)。圖3.1(b)~(f)中(zhong)深色(se)區為(wei)鐵素(su)(su)體(ti)(ti)(ti),淺色(se)區為(wei)奧(ao)氏體(ti)(ti)(ti)。奧(ao)氏體(ti)(ti)(ti)以鐵素(su)(su)體(ti)(ti)(ti)為(wei)基體(ti)(ti)(ti),呈帶狀或島狀分(fen)布(bu)于(yu)鐵素(su)(su)體(ti)(ti)(ti)上。隨著溫(wen)(wen)度的(de)升高,奧(ao)氏體(ti)(ti)(ti)晶粒尺寸變大。
利(li)用IAS圖像分(fen)析軟件測量(liang)(liang)(liang)并計算相(xiang)(xiang)比(bi)(bi)例(li),每(mei)個熱處理溫(wen)(wen)度(du)(du)下(xia)(xia)的(de)金(jin)相(xiang)(xiang)圖取(qu)8張計算,求取(qu)平均(jun)值(zhi)。表(biao)3.2給出了(le)利(li)用IAS圖像分(fen)析軟件計算得到(dao)不同固(gu)溶溫(wen)(wen)度(du)(du)溫(wen)(wen)度(du)(du)下(xia)(xia)2205雙相(xiang)(xiang)不銹鋼(gang)的(de)相(xiang)(xiang)比(bi)(bi)例(li)。1000℃時(shi),鐵素(su)體(ti)含(han)量(liang)(liang)(liang)為(wei)(wei)(wei)48.3%,隨(sui)著固(gu)溶溫(wen)(wen)度(du)(du)的(de)升(sheng)高,鐵素(su)體(ti)相(xiang)(xiang)含(han)量(liang)(liang)(liang)增加(jia),奧(ao)氏(shi)體(ti)相(xiang)(xiang)含(han)量(liang)(liang)(liang)下(xia)(xia)降,直到(dao)1200℃時(shi),鐵素(su)體(ti)含(han)量(liang)(liang)(liang)達到(dao)62.3%,奧(ao)氏(shi)體(ti)含(han)量(liang)(liang)(liang)僅(jin)占37.7%.這種鐵素(su)體(ti)與奧(ao)氏(shi)體(ti)隨(sui)固(gu)溶溫(wen)(wen)度(du)(du)的(de)變(bian)化(hua)(hua)規律(lv)前人的(de)研究(jiu)結果相(xiang)(xiang)一(yi)致。兩相(xiang)(xiang)比(bi)(bi)例(li)的(de)變(bian)化(hua)(hua)曲線如圖3.2所(suo)示,兩相(xiang)(xiang)與溫(wen)(wen)度(du)(du)的(de)關系呈線性變(bian)化(hua)(hua)。當固(gu)溶溫(wen)(wen)度(du)(du)約為(wei)(wei)(wei)1040℃時(shi),其相(xiang)(xiang)比(bi)(bi)例(li)為(wei)(wei)(wei)1:1。


因此(ci)在本(ben)實驗的(de)6個固溶溫度中,當固溶溫度為(wei)1050℃時,雙(shuang)相不銹鋼相比(bi)例最(zui)接近1:1。
采用顯(xian)微硬(ying)度(du)儀壓(ya)(ya)頭為菱形(xing)壓(ya)(ya)頭,荷載F為4.8N,分別測(ce)出菱形(xing)的兩個直徑d1和d2,根據下式計算(suan)顯(xian)微硬(ying)度(du):

所有(you)固溶(rong)(rong)溫度(du)(du)試樣(yang)均(jun)測5個點,最(zui)后求取平(ping)均(jun)值為個固溶(rong)(rong)溫度(du)(du)下2205雙相不銹鋼(gang)的顯(xian)微(wei)硬度(du)(du)值。顯(xian)微(wei)硬度(du)(du)值如(ru)表3.3所列(lie),顯(xian)微(wei)硬度(du)(du)隨(sui)固溶(rong)(rong)溫度(du)(du)的變(bian)化曲線如(ru)圖(tu)3.3所示。
從圖3.3可知,2205雙相不銹鋼的顯微硬度先下降,后上升。這主要是由于當溫度為1000℃時,鐵素體相中間夾雜著小塊狀的二次奧氏體,當溫度達到1050℃后,二次奧氏體含量減少,組織均勻化程度提高,硬度減小。在此之后,隨著固溶溫度的增加,奧氏體含量減少,具有體心立方結構的奧氏體相屬于軟軔相,具有面心立方結構的鐵素體是強硬相,因此材料顯微硬度值又升高。同樣對2507雙相不銹鋼進行不同溫度的固溶處理會導致2507雙相不銹鋼兩相組織的改變,進而導致其性能的差異,以下是2507雙相不銹鋼在不同溫度下固溶處理后的微觀組織。

2507雙相(xiang)(xiang)(xiang)(xiang)不(bu)銹鋼(gang)分別(bie)在1000℃、1050℃、1100℃、1150℃、1200℃下固(gu)溶(rong)(rong)(rong)(rong)0.5h后水冷的(de)(de)(de)金相(xiang)(xiang)(xiang)(xiang)組織如圖3.4所(suo)示(shi)。從圖3.4可以(yi)清晰地得(de)知當(dang)固(gu)溶(rong)(rong)(rong)(rong)溫(wen)(wen)(wen)度(du)為(wei)1000℃時(shi)(shi)(shi)鐵(tie)素體相(xiang)(xiang)(xiang)(xiang)與(yu)奧氏(shi)體相(xiang)(xiang)(xiang)(xiang)兩(liang)相(xiang)(xiang)(xiang)(xiang)相(xiang)(xiang)(xiang)(xiang)界處(chu)有(you)σ相(xiang)(xiang)(xiang)(xiang)析(xi)出,隨固(gu)溶(rong)(rong)(rong)(rong)處(chu)理溫(wen)(wen)(wen)度(du)升高(gao)到(dao)1050℃時(shi)(shi)(shi)σ相(xiang)(xiang)(xiang)(xiang)已(yi)經(jing)溶(rong)(rong)(rong)(rong)解。利用Image-Pro-Plus 圖像分析(xi)儀軟件6.0版(ban)測定的(de)(de)(de)相(xiang)(xiang)(xiang)(xiang)比例如圖3.5所(suo)示(shi)。從圖3.5能夠獲(huo)得(de)固(gu)溶(rong)(rong)(rong)(rong)熱(re)(re)處(chu)理溫(wen)(wen)(wen)度(du)的(de)(de)(de)增高(gao)會(hui)導致(zhi)σ析(xi)出相(xiang)(xiang)(xiang)(xiang)含量(liang)降低(di),當(dang)固(gu)溶(rong)(rong)(rong)(rong)熱(re)(re)處(chu)理溫(wen)(wen)(wen)度(du)大(da)于(yu)1050℃時(shi)(shi)(shi)σ相(xiang)(xiang)(xiang)(xiang)已(yi)經(jing)完(wan)全溶(rong)(rong)(rong)(rong)解。這是(shi)由(you)于(yu)固(gu)溶(rong)(rong)(rong)(rong)熱(re)(re)處(chu)理溫(wen)(wen)(wen)度(du)的(de)(de)(de)升高(gao)使(shi)鋼(gang)中(zhong)鐵(tie)素體α相(xiang)(xiang)(xiang)(xiang)量(liang)增多(duo),導致(zhi)σ相(xiang)(xiang)(xiang)(xiang)形成(cheng)元素Cr和Mo在鐵(tie)素體相(xiang)(xiang)(xiang)(xiang)中(zhong)的(de)(de)(de)濃度(du)降低(di),進(jin)而(er)導致(zhi)當(dang)固(gu)溶(rong)(rong)(rong)(rong)熱(re)(re)處(chu)理溫(wen)(wen)(wen)度(du)大(da)于(yu)1050℃時(shi)(shi)(shi)σ相(xiang)(xiang)(xiang)(xiang)的(de)(de)(de)形成(cheng)受到(dao)抑制。考慮到(dao)σ相(xiang)(xiang)(xiang)(xiang)硬且(qie)脆(cui),能夠大(da)幅度(du)減(jian)弱材料(liao)的(de)(de)(de)塑性(xing)與(yu)韌性(xing),并(bing)且(qie)σ相(xiang)(xiang)(xiang)(xiang)富(fu)Cr,很容(rong)易在其周圍(wei)產生(sheng)貧Cr區(qu)降低(di)DSS2507的(de)(de)(de)抗腐蝕(shi)性(xing)能,所(suo)以(yi)σ相(xiang)(xiang)(xiang)(xiang)為(wei)DSS2507析(xi)出相(xiang)(xiang)(xiang)(xiang)中(zhong)危害最大(da)的(de)(de)(de)相(xiang)(xiang)(xiang)(xiang),因此,在實(shi)際應(ying)用過程中(zhong)要(yao)想將2507雙相(xiang)(xiang)(xiang)(xiang)不(bu)銹鋼(gang)中(zhong)的(de)(de)(de)熱(re)(re)軋(ya)態σ相(xiang)(xiang)(xiang)(xiang)完(wan)全消除所(suo)選用的(de)(de)(de)固(gu)溶(rong)(rong)(rong)(rong)溫(wen)(wen)(wen)度(du)要(yao)不(bu)低(di)于(yu)1050℃。


圖3.4中深色組織(zhi)(zhi)是鐵(tie)(tie)(tie)素(su)體(ti)(ti)(ti)(ti)(ti)α相(xiang)(xiang)、淺色組織(zhi)(zhi)是奧氏(shi)(shi)(shi)(shi)(shi)體(ti)(ti)(ti)(ti)(ti)γ相(xiang)(xiang)。從圖3.4可(ke)(ke)知奧氏(shi)(shi)(shi)(shi)(shi)體(ti)(ti)(ti)(ti)(ti)γ相(xiang)(xiang)首(shou)先表現(xian)為長條狀,隨著固(gu)(gu)(gu)(gu)(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)處(chu)理(li)(li)溫(wen)(wen)度(du)(du)的升(sheng)高(gao)而逐(zhu)(zhu)(zhu)漸變(bian)短(duan),變(bian)成(cheng)島狀分布在基體(ti)(ti)(ti)(ti)(ti)鐵(tie)(tie)(tie)素(su)體(ti)(ti)(ti)(ti)(ti)上(shang)面。從圖3.5及表3.4中給出(chu)的相(xiang)(xiang)比例測(ce)量(liang)結果能夠獲(huo)得鋼中鐵(tie)(tie)(tie)素(su)體(ti)(ti)(ti)(ti)(ti)α相(xiang)(xiang)量(liang)隨固(gu)(gu)(gu)(gu)(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)熱(re)(re)處(chu)理(li)(li)溫(wen)(wen)度(du)(du)的升(sheng)高(gao)而上(shang)升(sheng),奧氏(shi)(shi)(shi)(shi)(shi)體(ti)(ti)(ti)(ti)(ti)γ相(xiang)(xiang)體(ti)(ti)(ti)(ti)(ti)積分數隨著固(gu)(gu)(gu)(gu)(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)溫(wen)(wen)度(du)(du)的上(shang)升(sheng)而下(xia)降,這是由于在較(jiao)高(gao)的固(gu)(gu)(gu)(gu)(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)溫(wen)(wen)度(du)(du)下(xia)2507雙相(xiang)(xiang)不銹鋼呈現(xian)出(chu)的組織(zhi)(zhi)為單一(yi)的鐵(tie)(tie)(tie)素(su)體(ti)(ti)(ti)(ti)(ti),隨固(gu)(gu)(gu)(gu)(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)熱(re)(re)處(chu)理(li)(li)溫(wen)(wen)度(du)(du)的降低鐵(tie)(tie)(tie)素(su)體(ti)(ti)(ti)(ti)(ti)逐(zhu)(zhu)(zhu)步(bu)轉(zhuan)化(hua)為奧氏(shi)(shi)(shi)(shi)(shi)體(ti)(ti)(ti)(ti)(ti)組織(zhi)(zhi),即固(gu)(gu)(gu)(gu)(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)熱(re)(re)處(chu)理(li)(li)溫(wen)(wen)度(du)(du)的升(sheng)高(gao)導致(zhi)奧氏(shi)(shi)(shi)(shi)(shi)體(ti)(ti)(ti)(ti)(ti)逐(zhu)(zhu)(zhu)漸轉(zhuan)變(bian)為鐵(tie)(tie)(tie)素(su)體(ti)(ti)(ti)(ti)(ti)組織(zhi)(zhi)。從圖3.5可(ke)(ke)以(yi)看出(chu)當(dang)固(gu)(gu)(gu)(gu)(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)熱(re)(re)處(chu)理(li)(li)溫(wen)(wen)度(du)(du)在1000~1050℃之間時奧氏(shi)(shi)(shi)(shi)(shi)體(ti)(ti)(ti)(ti)(ti)y相(xiang)(xiang)比例減小(xiao)的比較(jiao)緩(huan)慢,隨固(gu)(gu)(gu)(gu)(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)熱(re)(re)處(chu)理(li)(li)溫(wen)(wen)度(du)(du)的升(sheng)高(gao)奧氏(shi)(shi)(shi)(shi)(shi)體(ti)(ti)(ti)(ti)(ti)γ相(xiang)(xiang)含(han)量(liang)減少的趨勢加快,這是因為2507雙相(xiang)(xiang)不銹鋼中的氮元素(su)是奧氏(shi)(shi)(shi)(shi)(shi)體(ti)(ti)(ti)(ti)(ti)形成(cheng)元素(su),在較(jiao)低固(gu)(gu)(gu)(gu)(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)溫(wen)(wen)度(du)(du)下(xia)抑制(zhi)了奧氏(shi)(shi)(shi)(shi)(shi)體(ti)(ti)(ti)(ti)(ti)相(xiang)(xiang)向鐵(tie)(tie)(tie)素(su)體(ti)(ti)(ti)(ti)(ti)相(xiang)(xiang)的轉(zhuan)變(bian),而固(gu)(gu)(gu)(gu)(gu)溶(rong)(rong)(rong)(rong)(rong)(rong)熱(re)(re)處(chu)理(li)(li)溫(wen)(wen)度(du)(du)的升(sheng)高(gao)會使N元素(su)穩定奧氏(shi)(shi)(shi)(shi)(shi)體(ti)(ti)(ti)(ti)(ti)相(xiang)(xiang)的作用逐(zhu)(zhu)(zhu)漸減弱,進而導致(zhi)奧氏(shi)(shi)(shi)(shi)(shi)體(ti)(ti)(ti)(ti)(ti)γ相(xiang)(xiang)向鐵(tie)(tie)(tie)素(su)體(ti)(ti)(ti)(ti)(ti)α相(xiang)(xiang)轉(zhuan)變(bian)速度(du)(du)加快。
2507雙(shuang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)不銹(xiu)鋼中(zhong)(zhong)的(de)(de)(de)(de)奧(ao)氏(shi)體(ti)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)和鐵素(su)體(ti)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)這兩(liang)種相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)的(de)(de)(de)(de)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比例(li)(li)(li)主要(yao)受固(gu)(gu)(gu)(gu)溶(rong)處理(li)工藝以(yi)(yi)及(ji)自(zi)身(shen)化學成分(fen)的(de)(de)(de)(de)影(ying)響,當(dang)(dang)鋼的(de)(de)(de)(de)主要(yao)化學成分(fen)確定時,則兩(liang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比例(li)(li)(li)與固(gu)(gu)(gu)(gu)溶(rong)處理(li)制(zhi)度(du)(du)(du)有著(zhu)密切(qie)聯系。DSS2507的(de)(de)(de)(de)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比例(li)(li)(li)又影(ying)響著(zhu)其自(zi)身(shen)的(de)(de)(de)(de)性能(neng)(neng)(neng),其塑性隨著(zhu)鐵素(su)體(ti)含(han)量的(de)(de)(de)(de)增多而(er)減弱(ruo)、耐應(ying)力(li)腐蝕破裂(lie)能(neng)(neng)(neng)力(li)隨著(zhu)奧(ao)氏(shi)體(ti)含(han)量升高而(er)減弱(ruo),進(jin)而(er)認為當(dang)(dang)鐵素(su)體(ti)α相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)跟(gen)奧(ao)氏(shi)體(ti)γ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)這兩(liang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比例(li)(li)(li)接近1:1時雙(shuang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)不銹(xiu)鋼的(de)(de)(de)(de)綜合(he)性能(neng)(neng)(neng)最(zui)佳,有較(jiao)好(hao)的(de)(de)(de)(de)抗腐蝕能(neng)(neng)(neng)力(li)以(yi)(yi)及(ji)較(jiao)優(you)的(de)(de)(de)(de)力(li)學性能(neng)(neng)(neng)。從圖3.5可知固(gu)(gu)(gu)(gu)溶(rong)熱處理(li)溫(wen)(wen)度(du)(du)(du)在1050~1100℃之(zhi)間時可以(yi)(yi)使鋼中(zhong)(zhong)的(de)(de)(de)(de)兩(liang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)組織(zhi)比例(li)(li)(li)達到1:1,本實驗(yan)中(zhong)(zhong)所(suo)選(xuan)用的(de)(de)(de)(de)5種固(gu)(gu)(gu)(gu)溶(rong)溫(wen)(wen)度(du)(du)(du)中(zhong)(zhong)1050℃時鐵素(su)體(ti)α相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)跟(gen)奧(ao)氏(shi)體(ti)γ相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)比例(li)(li)(li)最(zui)接近1:1,進(jin)而(er)可以(yi)(yi)認為選(xuan)擇較(jiao)優(you)的(de)(de)(de)(de)固(gu)(gu)(gu)(gu)溶(rong)熱處理(li)溫(wen)(wen)度(du)(du)(du)使DSS2507中(zhong)(zhong)的(de)(de)(de)(de)兩(liang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)含(han)量比例(li)(li)(li)達到1:1是有可能(neng)(neng)(neng)的(de)(de)(de)(de),在實際應(ying)用過程(cheng)中(zhong)(zhong)為了使2507雙(shuang)相(xiang)(xiang)(xiang)(xiang)(xiang)(xiang)不銹(xiu)鋼獲得較(jiao)好(hao)的(de)(de)(de)(de)綜合(he)性能(neng)(neng)(neng),進(jin)行固(gu)(gu)(gu)(gu)溶(rong)處理(li)時選(xuan)取的(de)(de)(de)(de)固(gu)(gu)(gu)(gu)溶(rong)溫(wen)(wen)度(du)(du)(du)應(ying)該(gai)在1050~1100℃之(zhi)間。
2507雙(shuang)相(xiang)不(bu)(bu)銹(xiu)(xiu)鋼(gang)(gang)(gang)分別在(zai)1000℃、1050℃、1100℃、1150℃、1200℃固(gu)(gu)(gu)溶(rong)(rong)(rong)0.5h后(hou)(hou)水冷的(de)(de)(de)(de)(de)硬(ying)度(du)(du)(du)值(zhi)如圖3.6所示。從圖3.6可(ke)知DSS2507的(de)(de)(de)(de)(de)硬(ying)度(du)(du)(du)隨(sui)固(gu)(gu)(gu)溶(rong)(rong)(rong)處理(li)(li)(li)溫(wen)(wen)(wen)度(du)(du)(du)的(de)(de)(de)(de)(de)升(sheng)(sheng)高(gao)(gao)先減小后(hou)(hou)變(bian)大(da)呈(cheng)曲(qu)線變(bian)化。在(zai)1000~1050℃溫(wen)(wen)(wen)度(du)(du)(du)范圍內鋼(gang)(gang)(gang)的(de)(de)(de)(de)(de)硬(ying)度(du)(du)(du)隨(sui)固(gu)(gu)(gu)溶(rong)(rong)(rong)熱處理(li)(li)(li)溫(wen)(wen)(wen)度(du)(du)(du)的(de)(de)(de)(de)(de)增高(gao)(gao)而逐漸(jian)(jian)減小,1050~1200℃范圍內隨(sui)固(gu)(gu)(gu)溶(rong)(rong)(rong)熱處理(li)(li)(li)溫(wen)(wen)(wen)度(du)(du)(du)的(de)(de)(de)(de)(de)上升(sheng)(sheng)硬(ying)度(du)(du)(du)又(you)(you)漸(jian)(jian)漸(jian)(jian)變(bian)大(da),且(qie)1050℃時(shi)DSS2507的(de)(de)(de)(de)(de)硬(ying)度(du)(du)(du)表現為(wei)最(zui)小。從3.2.1節(jie)分析可(ke)知當固(gu)(gu)(gu)溶(rong)(rong)(rong)溫(wen)(wen)(wen)度(du)(du)(du)為(wei)1000℃時(shi)在(zai)鐵(tie)素(su)體(ti)(ti)和奧氏體(ti)(ti)相(xiang)界(jie)處有(you)σ相(xiang)析出,σ相(xiang)是(shi)一種硬(ying)而脆(cui)的(de)(de)(de)(de)(de)相(xiang),能夠提高(gao)(gao)雙(shuang)相(xiang)不(bu)(bu)銹(xiu)(xiu)鋼(gang)(gang)(gang)的(de)(de)(de)(de)(de)硬(ying)度(du)(du)(du)值(zhi),所以1000℃下鋼(gang)(gang)(gang)有(you)較高(gao)(gao)的(de)(de)(de)(de)(de)硬(ying)度(du)(du)(du),而σ相(xiang)會隨(sui)固(gu)(gu)(gu)溶(rong)(rong)(rong)熱處理(li)(li)(li)溫(wen)(wen)(wen)度(du)(du)(du)的(de)(de)(de)(de)(de)升(sheng)(sheng)高(gao)(gao)而漸(jian)(jian)漸(jian)(jian)溶(rong)(rong)(rong)解到基體(ti)(ti)中,DSS2507的(de)(de)(de)(de)(de)硬(ying)度(du)(du)(du)有(you)下降的(de)(de)(de)(de)(de)趨勢;同時(shi)又(you)(you)由(you)于固(gu)(gu)(gu)溶(rong)(rong)(rong)熱處理(li)(li)(li)溫(wen)(wen)(wen)度(du)(du)(du)的(de)(de)(de)(de)(de)增高(gao)(gao)導致(zhi)鋼(gang)(gang)(gang)中的(de)(de)(de)(de)(de)鐵(tie)素(su)體(ti)(ti)相(xiang)量增加而奧氏體(ti)(ti)相(xiang)量降低,在(zai)室(shi)溫(wen)(wen)(wen)下鐵(tie)素(su)體(ti)(ti)是(shi)體(ti)(ti)心(xin)立(li)方(fang)結構(gou)(bcc)奧氏體(ti)(ti)是(shi)面心(xin)立(li)方(fang)結構(gou)(fcc),前者硬(ying)度(du)(du)(du)要高(gao)(gao)于后(hou)(hou)者,因此在(zai)鐵(tie)素(su)體(ti)(ti)含量逐漸(jian)(jian)升(sheng)(sheng)高(gao)(gao)的(de)(de)(de)(de)(de)情況下鋼(gang)(gang)(gang)的(de)(de)(de)(de)(de)硬(ying)度(du)(du)(du)也逐漸(jian)(jian)升(sheng)(sheng)高(gao)(gao),即隨(sui)著固(gu)(gu)(gu)溶(rong)(rong)(rong)溫(wen)(wen)(wen)度(du)(du)(du)的(de)(de)(de)(de)(de)升(sheng)(sheng)高(gao)(gao)2507 雙(shuang)相(xiang)不(bu)(bu)銹(xiu)(xiu)鋼(gang)(gang)(gang)的(de)(de)(de)(de)(de)硬(ying)度(du)(du)(du)呈(cheng)升(sheng)(sheng)高(gao)(gao)的(de)(de)(de)(de)(de)趨勢。綜上所述,隨(sui)固(gu)(gu)(gu)溶(rong)(rong)(rong)溫(wen)(wen)(wen)度(du)(du)(du)從1000℃上升(sheng)(sheng)到1200℃,2507雙(shuang)相(xiang)不(bu)(bu)銹(xiu)(xiu)鋼(gang)(gang)(gang)硬(ying)度(du)(du)(du)呈(cheng)先降低后(hou)(hou)升(sheng)(sheng)高(gao)(gao)的(de)(de)(de)(de)(de)變(bian)化趨勢。


